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Laboratory I

Code:

TPD006

Sigla:

Áreas Científicas
Classificação	Área Científica
OFICIAL	Química

Ocorrência: 2022/2023 - 1S

Ativa?	Yes
Unidade Responsável:	Departamento de Engenharia Química e Biológica
Curso/CE Responsável:	Undergraduate in Oil & Gas Technologies

Ciclos de Estudo/Cursos

Sigla	Nº de Estudantes	Plano de Estudos	Anos Curriculares	Créditos UCN	Créditos ECTS	Horas de Contacto	Horas Totais
TPD	42	Study Plan	1	-	5	60	135

Docência - Responsabilidades

Docente	Responsabilidade
Rui Manuel Marques Antunes

Docência - Horas

Practical and Laboratory:

3,00

Type	Docente	Turmas	Horas
Practical and Laboratory	Totais	3	9,00
	Joana Luís Refoios de Noronha Tudella		3,00
	Catarina Alexandra Veríssimo Esteves		6,00

Língua de trabalho

Portuguese

Objetivos

The purpose of discipline is to provide skills training in basic operations of chemical laboratory. After completed the course, students should have acquired the following competencies:

- 1. Ability to analyze data analytical and experimental results.

- 2. Interpreting the sources of uncertainty and the ways of propagation.

- 3. Competence in handling analytical glassware, analytical equipment, and reagents in the laboratory.

Resultados de aprendizagem e competências

Does not apply.

Modo de trabalho

Presencial

Pré-requisitos (conhecimentos prévios) e co-requisitos (conhecimentos simultâneos)

Does not apply.

Programa

1. Safety Practices in the Chemistry Lab. 2. Measurement and handling numbers. 3. Types of Solutions and concentration units. 4. Techniques of handling analytical glassware and analytical equipment. 5. Separation Processes (filtration, decantation, extraction). 6. Techniques for purification of compounds (crystallization, distillation, chromatography, etc.).

Bibliografia Obrigatória

Raymond Chang; Chemistry,, Williams College, 2005

Métodos de ensino e atividades de aprendizagem

The modular course consists of two preliminary lectures and eight experiments performed by teams of two students each. The lab work is organized as follows:

1- Preparing for the experiment. The students should read and understand the laboratory protocol and read suggested reference materials prior to the lab session. In addition, some lab session time will usually be devoted to a discussion of the theory concern the experiment.

2- Running the experiment. Each team is responsible for conducting each experiment under supervision of instructor. 3- End of the experiment. Preliminary discussion of the experimental outcomes with instructor. 4- Report.

The final grade will be determined by proportionally weighting performance in the following assessment elements:

full reports (60 %); Individual practical examination (25%); participation in lab work as evaluated by instructor (15%).

Tipo de avaliação

Distributed evaluation without final exam

Componentes de Avaliação

Designation	Peso (%)
Participação presencial	15,00
Teste	25,00
Trabalho laboratorial	60,00
Total:	100,00

Componentes de Ocupação

Designation	Tempo (Horas)
Frequência das aulas	45,00
Total:	45,00

Obtenção de frequência

Does not apply.

Fórmula de cálculo da classificação final

CF = 0.60 x (arithmetic mean of the reports) + 0.25 x practical exam + 0.15 performance in the laboratory

Provas e trabalhos especiais

Does not apply.

Trabalho de estágio/projeto

Does not apply.

Avaliação especial (TE, DA, ...)

Does not apply.

Melhoria de classificação

Does not apply.

Observações

Does not apply.

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