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Instrumental Methods of Analysis C

Code:

TLQE016

Sigla:

MIAC

Áreas Científicas
Classificação	Área Científica
CNAEF	Chemical process technology

Ocorrência: 2019/2020 - 1S

Ativa?	Yes
Unidade Responsável:	Química
Curso/CE Responsável:

Ciclos de Estudo/Cursos

Sigla	Nº de Estudantes	Plano de Estudos	Anos Curriculares	Créditos UCN	Créditos ECTS	Horas de Contacto	Horas Totais
TLQBE	5	Study Plan	2	-	7,5	75	202,5

Língua de trabalho

Portuguese - Suitable for English-speaking students

Objetivos

At the end of this CU, the student must:
- Plan and carry out advanced laboratory techniques.
- Understand and use quality control in the results of analytical measurements.
- Know the instrumentation, the physical-chemical principle of each analytical method, and its advantages and disadvantages.
- Apply calibration methods.
- Interpret the results of analytical chemistry and acquire critical skills and integration of knowledge in laboratory work.

Resultados de aprendizagem e competências

Not applicable

Modo de trabalho

Presencial

Programa

1. Qualitative Analysis and Quantitative Analysis.
2. Optical Methods (atomic and molecular absorption - UV/VIS; flame photometry; atomic emission, FTIR, ICP; Fluorescence, Phosphorescence).
3. Mass spectrometry.
4. Electroanalytical methods (potentiometric, voltammetric, coulimetric and electrogravimetric methods).
5. X-ray diffraction.
6. Nuclear Magnetic Resonance.
7. Chromatographic methods (HPLC, GC, SEC, hyphenated techniques, etc.).

Bibliografia Obrigatória

Harris, D.C.; Quantitative Chemical Analysis, W.H. Freeman and Company, New York, 8th Edition, 2010
Skoog, D.A., West, D.M., Holler, F.J., Crouch, S.R.; Fundamentals of Analytical Chemistry, Brooks/ColeThomson Learning, Belmont, 8th Edition, 2004
Skoog, D.A., West, D.M., Holler, F.J., Crouch, S.R.; Principles of Instrumental Analysis, Thomson Brooks/Cole, Belmont, 6th Edition, International Student Edition, 2007
Gonçalves, M.L.S.S.; Métodos Instrumentais para a Análise de Soluções/Análise Quantitativa, Fundação Calouste Gulbenkian, Lisboa, 4ª Edição, 2001
Romão, M.S.; Análise Química, Técnico Lisboa, 2013

Métodos de ensino e atividades de aprendizagem

In the theoretical classes, the expository technique is used, stimulating the students' reasoning and critical spirit.

In practical or laboratory classes, students solve exercises and perform laboratory work independently under the supervision of the professor.

The assessment consists of 50% for the theoretical component (tests or exam) and 50% for the practical component (Classroom Context, Laboratory Notebook and Reports).

Tipo de avaliação

Distributed evaluation with final exam

Componentes de Avaliação

Designation	Peso (%)
Teste	50,00
Trabalho laboratorial	50,00
Total:	100,00

Componentes de Ocupação

Designation	Tempo (Horas)
Estudo autónomo	127,50
Frequência das aulas	75,00
Total:	202,50

Obtenção de frequência

Mandatory attendance, as a condition of access to continuous assessment, refers exclusively to laboratory classes, that is, the student must perform all the experimental work proposed in the laboratory, which implies that if a student misses a laboratory class, he/she will have to do the missing work in a recovery class at the end of the semester.

Fórmula de cálculo da classificação final

Evaluation in the academic period:

25% Test 1 + 25% Test 2 + 10% Classroom Context + 15% Laboratory Notebook + 25% Reports.

Exam (all seasons):

50% Exam + 10% Classroom Context + 15% Laboratory Notebook + 25% Reports.


A student must obtain a grade equal to or greater than 9.5 in the weighted average of the Tests.

In Assessment by exam of 1st/2nd season, midterm or special season, the minimum grade in the exam is 9.5 values.


In terms of individual assessment of group work, it is indicated that:

- The student who signs the work and does not appear in its oral discussion, can be assigned a null classification in the discussion (weight of 20% in the final classification of the work).

- Students from the same group may be given a different classification during the discussion, based on the mastery of the content of the work carried out.