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Instrumental Methods of Analysis

Code:

BIOT106

Sigla:

MIA I

Áreas Científicas
Classificação	Área Científica
OFICIAL	Química

Ocorrência: 2023/2024 - 1S

Ativa?	Yes
Página Web:	https://moodle.ips.pt/2324/course/view.php?id=532
Unidade Responsável:	Departamento de Engenharia Química e Biológica
Curso/CE Responsável:	Undergraduate in Biotechnology

Ciclos de Estudo/Cursos

Sigla	Nº de Estudantes	Plano de Estudos	Anos Curriculares	Créditos UCN	Créditos ECTS	Horas de Contacto	Horas Totais
BIOT	54	Study Plan	2	-	5	60	135

Língua de trabalho

Portuguese - Suitable for English-speaking students

Objetivos

The objectives of this CU are:
To be able to use optical, electroanalytical, chromatographic methods, etc.;
To identify advantages and limitations for each technique;
To describe the functioning of each technique devices;
To use these devices knowing the best way of profiting from its potentialities;
Knowing the best technique to use in each situation (expected results and cost);
To identify and apply the preliminary steps that allowed an efficient use of each technique.

Resultados de aprendizagem e competências

Not Applicable

Modo de trabalho

Presencial

Programa

1. Qualitative and Quantitative analyses.
2. Optical Methods (atomic and molecular absorption – UV/VIS; flame photometry; atomic emission, ICP; Fluorescence, Phosphorescence).
3. Mass Spectrometry.
4. Electroanalytical Methods (Potentiometric methods, Voltammetric, Coulometric and Electrogravimetric methods).
5. RX Diffraction.
6. Chromatographic Methods (HPLC, GC, SEC, hyphenated techniques, etc.).

Bibliografia Obrigatória

M.L.S. Gonçalves; Métodos Instrumentais para a Análise de Soluções, Análise Quantitativa, Fundação Calouste Gulbenkian, 4th. ed., 2001
D.C. Harris; Quantitative Chemical Analysis, W.H. Freeman and Co., 6th ed., 2003
D.A. Skoog, F.J. Holler, T.A. Nieman; Principles of Instrumental Analysis, Saunders College Publishing, 5th ed., 1998

Métodos de ensino e atividades de aprendizagem

Lecture or applied theory classes will be administered, using a lecture-based approach, using for that purpose slides or overhead projector presentations. The classes will be planning with the aim to stimulate interest, reasoning and critical spirit of the students. In the applied theory classes the students will autonomously resolve the exercises.

The continuous evaluation consists of 20% for the presentation/discussion of a scientific work and 80% for two tests. The exam evaluation consists of 20% for the presentation/discussion of a scientific work and 80% for the exam, or 100% exam.

Tipo de avaliação

Distributed evaluation with final exam

Componentes de Avaliação

Designation	Peso (%)
Apresentação/discussão de um trabalho científico	20,00
Teste	80,00
Total:	100,00

Componentes de Ocupação

Designation	Tempo (Horas)
Apresentação/discussão de um trabalho científico	12,00
Estudo autónomo	70,50
Frequência das aulas	52,50
Total:	135,00

Obtenção de frequência

Not Applicable

Fórmula de cálculo da classificação final

Continuous Evaluation:
FM=40% Test 1 + 40% Test 2 + 20% Presentation/discussion of a scientific paper.

Minimum grade of 9.5 points in the weighted average of the tests.

Exam Evaluation (all seasons):
FM=100% Exam or 80% Exam + 20% Presentation/discussion of a scientific paper – the best of the two options will be applied.

Minimum exam grade is 9.5 points.

- The student who signs the work and does not appear in its oral presentation/discussion, can be assigned a null classification in that presentation (weight of 50% in the final classification of the work). A different classification may be given to students in the same group based on the commitment shown, the quality of the oral presentation and the domain of the theme.

- The two tests and the presentation/discussion of a scientific paper are compulsory as a condition of continuous assessment.