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Separation Processes IIB

Code: BIOT157     Sigla: PS IIB

Áreas Científicas
Classificação Área Científica
OFICIAL Processos em Engenharia Química e Biológica

Ocorrência: 2023/2024 - 1S

Ativa? Yes
Unidade Responsável: Departamento de Engenharia Química e Biológica
Curso/CE Responsável: Undergraduate in Biotechnology

Ciclos de Estudo/Cursos

Sigla Nº de Estudantes Plano de Estudos Anos Curriculares Créditos UCN Créditos ECTS Horas de Contacto Horas Totais
BIOT 68 Study Plan 3 - 5 60 135

Docência - Responsabilidades

Docente Responsabilidade
Ana Cláudia Cavaco de Sousa Coelho

Docência - Horas

Theorethical: 2,00
Theorethical and Practical : 1,50
Type Docente Turmas Horas
Theorethical Totais 1 2,00
Ana Cláudia Cavaco de Sousa Coelho 2,00
Theorethical and Practical Totais 2 3,00
Ana Cláudia Cavaco de Sousa Coelho 1,50

Língua de trabalho

Portuguese
Obs.: Português suitable for english speaking students

Objetivos

The curricular unit of Separation Process II B aims to equip students with knowledge of membrane separation, adsorption and ion exchange chromatography. At the same time it is intended that students acquire the knowledge to analyze and to scale up the separation equipment.



After the approval of this course, students should be able to: 1) Identify and apply advanced separation processes such as distil ation optimized, supercritical extraction, membrane separation, adsorption, exchange and ion chromatography. 2) Know to scale up equipment for separation processes studied to simpler and complex mixtures. 3) Analyze and study the operation of this equipment.

Resultados de aprendizagem e competências

Not applicable

Modo de trabalho

Presencial

Programa

1. Sorption processes: adsorption, chromatography and ion exchange. Kinetics and equilibrium. Equilibrium. Fixed beds. Linear theories. Solute movement theory. Application to chromatography and adsorption. Dispersion mechanisms in columns.
2. Chromatography processes: adsorption chromatography, ion exchange, molecular exclusion, affinity, reverse phase, covalent, hydrophobic interaction. Operating conditions: Darcy, Kozeny and Ergun equations. Scale-up. Large-scale chromatographic processes.
3. Filtration at constant flow and pressure. Filter sizing.
4. Membrane processes. Processes under pressure. Transport models. Concentration polarisation. Modes of operation. "Membrane fouling. Selection and sizing. Synthesising sequences of operations. Liquid membranes.

Bibliografia Obrigatória

Raja, Ghosh; Principles of Bioseparations Engineering, McMaster University, World Scientific Publishing, 2006. ISBN: 981-256-892-1

Bibliografia Complementar

Carlos, A. V. Costa, Joaquim S. Cabral; Chromatographic and Membrane Processes in Biotechnology, Springer Science + Business Media. ISBN: 978-94-010-5535-2
J. D. Seader, Ernest J. Henley, D. Keith Roper; Separation Process Principles, Wiley, John Wiley & Sons, 2011

Métodos de ensino e atividades de aprendizagem

Theoretical material will be presented to promote the involvement and participation of all students by developing their reasoning skills and stimulating their critical thinking. Materials about the subjects lectured will be available for consultations on Moodle. It will be proposed to carry out a group work to deepen the application of one of the processes learned during theorical lessons. Some guided technical visits are foreseen to consolidate the topics taught. At any time, students can contact the teacher through the same platform.


The assessment consists of 10% for the accomplishment of three exercises proposed throughout the semester, 10% for group work and 80% of the theoretical component.

In the assessment regime by final exam, 10% is considered for group work and 90% for the classification of the exam.

Tipo de avaliação

Distributed evaluation with final exam

Componentes de Avaliação

Designation Peso (%)
Teste 80,00
Trabalho escrito 20,00
Total: 100,00

Componentes de Ocupação

Designation Tempo (Horas)
Estudo autónomo 55,00
Frequência das aulas 60,00
Trabalho escrito 20,00
Total: 135,00

Obtenção de frequência

In continuous assessment, all assessment elements are classified between 0 and 20 values and their weighted average according to the percentage coefficients indicated should be 9.5 values.



The non-realization of an element assumes a zero in its classification.

Fórmula de cálculo da classificação final

Continuous assessment

0.8*average of the two tests + 0.10*group work (written work) + 0.10*regular exercises


Minimum mark for the arithmetic average of the two tests is 8 values

Exam

100% exam or 0.90*exam + 0.10*group work

Minimum exam mark is 9 values
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